注射器,之后在移動phaseor其他合適的解決方案,解散,被色譜分離化合物注射施行本科生流動相,無論是手動注射器或注射器循環(huán),orautomatically通過自動進樣器.后者包括一個轉(zhuǎn)盤或機架holdsample小瓶與具有可刺穿的隔膜或塞子和aninjection設(shè)備從小瓶轉(zhuǎn)移樣品到它被裝入色譜儀校準,固定volumeloop片斷.一些自動采樣器可以beprogrammed來控制樣品的體積,注射劑和循環(huán)rinsecycles的數(shù)量,注射之間的時間間隔,以及其他操作變量.
注射器可用于手動injectionof樣品通過隔膜時柱頭壓力小于70atmospheres (大約1000PSI ) .在較高壓力下的噴射閥是essential.Some閥系統(tǒng)包括thatis充滿試驗溶液轉(zhuǎn)移到流動相中的柱校準循環(huán).Inother系統(tǒng),測試溶液通過注射器轉(zhuǎn)移至腔和thenswitched入流動相.非常感謝,請問有沒有更好的,上面的似乎不太對頭,有些很難理解
求高人幫忙翻譯一下,非常感謝
求高人幫忙翻譯一下,非常感謝
Injectors-After dissolution in mobile phaseor other suitable solution, compounds to be chromatographed are injected intothe mobile phase, either manually by syringe or loop injectors, orautomatically by autosamplers. The latter consist of a carousel or rack to holdsample vials with tops that have a pierceable septum or stopper and aninjection device to transfer sample from the vials to a calibrated, fixed-volumeloop from which it is loaded into the chromatograph. Some auto-samplers can beprogrammed to control sample volume, the number of injections and loop rinsecycles, the interval between injections, and other operating variables.
A syringe can be used for manual injectionof samples through a septum when column head pressures are less than 70atmospheres(about 1000psi). At higher pressure an injection valve is essential.Some valve systems incorporate a calibrated loop thatis filled with test solution for transfer to the column in the mobile phase. Inother systems, test solution is transferred to a cavity by syringe and thenswitched into the mobile phase.
Injectors-After dissolution in mobile phaseor other suitable solution, compounds to be chromatographed are injected intothe mobile phase, either manually by syringe or loop injectors, orautomatically by autosamplers. The latter consist of a carousel or rack to holdsample vials with tops that have a pierceable septum or stopper and aninjection device to transfer sample from the vials to a calibrated, fixed-volumeloop from which it is loaded into the chromatograph. Some auto-samplers can beprogrammed to control sample volume, the number of injections and loop rinsecycles, the interval between injections, and other operating variables.
A syringe can be used for manual injectionof samples through a septum when column head pressures are less than 70atmospheres(about 1000psi). At higher pressure an injection valve is essential.Some valve systems incorporate a calibrated loop thatis filled with test solution for transfer to the column in the mobile phase. Inother systems, test solution is transferred to a cavity by syringe and thenswitched into the mobile phase.
英語人氣:456 ℃時間:2020-07-29 09:15:18
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